短波近红外光谱法分析酒中乙醇含量初探

使用短波近红外光谱和多变量校正技术快速准确地测定酒中乙醇含量,研究了纯水、乙醇以及乙醇和水混合体系的光谱特征。用多元线性回归(MLR)和主成分回归(PCR)分析了数据。该法分析酒样具有方便、快速的优点。     

Prediction Regions for Bivariate Extreme Events

This paper suggests using a mixture of parametric and non‐parametric methods to construct prediction regions in bivariate extreme‐value problems. The non‐parametric part of the technique is used to estimate the dependence function, or copula, and the parametric part is employed to estimate the marginal distributions. A bootstrap calibration argument is suggested for reducing coverage error. This combined approach is compared with a more parametric one, relative to which it has the advantages of being more flexible and simpler to implement. It also enjoys these features relative to predictive likelihood methods. The paper shows how to construct both compact and semi‐infinite bivariate prediction regions, and it treats the problem of predicting the value of one component conditional on the other. The methods are illustrated by application to Australian annual maximum temperature data.     

Idle thoughts of a ‘well‐calibrated’ Bayesian in clinical drug development

The use of Bayesian approaches in the regulated world of pharmaceutical drug development has not been without its difficulties or its critics. The recent Food and Drug Administration regulatory guidance on the use of Bayesian approaches in device submissions has mandated an investigation into the operating characteristics of Bayesian approaches and has suggested how to make adjustments in order that the proposed approaches are in a sense calibrated. In this paper, I present examples of frequentist calibration of Bayesian procedures and argue that we need not necessarily aim for perfect calibration but should be allowed to use procedures, which are well‐calibrated, a position supported by the guidance. Copyright © 2016 John Wiley & Sons, Ltd.     

抽样调查中的校准估计法

本文梳理总结了校准估计法自首次提出以来的研究成果。理论方法的发展集中在最短距离法、工具向量法和模型校准法三种校准方法的研究上;方法应用的发展体现在对简单参数和复杂参数的校准估计上。对小域估计、无回答、二重抽样等特定抽样问题和总体分位数、总体方差估计中校准估计法的具体应用作了重点梳理介绍。对校准估计法的理论和应用研究前景作了展望。     

Accurate Confidence Interval Estimation of Small Area Parameters Under the Fay–Herriot Model

Small area estimation has long been a popular and important research topic due to its growing demand in public and private sectors. We consider here the basic area level model, popularly known as the Fay–Herriot model. Although much of current research is predominantly focused on second order unbiased estimation of mean squared prediction errors, we concentrate on developing confidence intervals (CIs) for the small area means that are second order correct. The corrected CI can be readily implemented, because it only requires quantities that are already estimated as part of the mean squared error estimation. We extend the approach to a CI for the difference of two small area means. The findings are illustrated with a simulation study.     

Linear calibra and conditional inference

Approximate conditional inference is developed for the linear calibration problem. It is shown that this problem can be transformed so that the primary parameter is an angle, the nuisance parameter is a radial distance, and the density is rotationally symmetric. Were the nuisance parameter known, exact location confidence intervals would be available by location of structural arguments. A confidence distribution is used to average out the nuisance parameter yielding an approximate confidence interval that involves a precision indicator derived from the radial distance. Some difficulties with the ordinary solution are avoided by the conditional procedure.     

Estimation and Testing in Elliptical Functional Measurement Error Models

The purpose of this article is to investigate estimation and hypothesis testing by maximum likelihood and method of moments in functional models within the class of elliptical symmetric distributions. The main results encompass consistency and asymptotic normality of the method of moments estimators. Also, the asymptotic covariance matrix of the maximum likelihood estimator is derived, extending some existing results in elliptical distributions. A measure of asymptotic relative efficiency is reported. Wald-type statistics are considered and numerical results obtained by Monte Carlo simulation to investigate the performance of estimators and tests are provided for Student-t and contaminated normal distributions. An application to a real dataset is also included.     

On Confidence Intervals for Process Capability Indices in a One-Way Random Model

In this article, we investigated the bootstrap calibrated generalized confidence limits for process capability indices C _pk for the one-way random effect model. Also, we derived Bissell's approximation formula for the lower confidence limit using Satterthwaite's method and calculated its coverage probabilities and expected values. Then we compared it with standard bootstrap (SB) method and generalized confidence interval method. The simulation results indicate that the confidence limit obtained offers satisfactory coverage probabilities. The proposed method is illustrated with the help of simulation studies and data sets.     

Calibration of the estimators of variance

This investigation suggests new techniques to calibrate estimators of variance. Estimators of the variance of simple mean, ratio and regression estimators under different sampling schemes are shown to be special cases of the proposed calibration techniques. The approach has more practical use due to recent advances in programming techniques and computational speed. An empirical study has been carried out to address the properties of these proposed strategies.     

Unconditional empirical likelihood approach for analytic use of public survey data

Modeling survey data often requires having the knowledge of design and weighting variables. With public-use survey data, some of these variables may not be available for confidentiality reasons. The proposed approach can be used in this situation, as long as calibrated weights and variables specifying the strata and primary sampling units are available. It gives consistent point estimation and a pivotal statistics for testing and confidence intervals. The proposed approach does not rely on with-replacement sampling, single-stage, negligible sampling fractions, or noninformative sampling. Adjustments based on design effects, eigenvalues, joint-inclusion probabilities or bootstrap, are not needed. The inclusion probabilities and auxiliary variables do not have to be known. Multistage designs with unequal selection of primary sampling units are considered. Nonresponse can be easily accommodated if the calibrated weights include reweighting adjustment for nonresponse. We use an unconditional approach, where the variables and sample are random variables. The design can be informative.