高压微波催化合成肉桂酸甲酯 |
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引用本文: | 凌绍明,谭绍炳,余万荣.高压微波催化合成肉桂酸甲酯[J].百色学院学报,2002,15(3):41-43. |
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作者姓名: | 凌绍明 谭绍炳 余万荣 |
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作者单位: | 广西右江民族师专,化学系,广西,百色,533000 |
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摘 要: | 在硫酸铁铵的催化下 ,利用高压微波技术 ,快速合成了肉桂酸甲酯。最佳反应条件为 :甲醇和肉桂酸的摩尔比为 5 :1,催化剂用量为 2 .0g ,微波时间为 3min ,微波功率为 72 9W ,产率达93.8%。
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关 键 词: | 高压微波 肉桂酸甲酯 合成 催化 硫酸铁铵 |
文章编号: | 1008-8113(2002)03-0041-03 |
修稿时间: | 2002年5月16日 |
Synthesis of Methyl Cinnamate with Catalyst and High pressure Microwave |
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Authors: | Ling Shao-Ming Tan Shao-Bing Yu Wan-Rong |
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Abstract: | The methyl cinnamate is synthesized fastly with the technigue of high pressure microwave, and the catalyst of ammonium ferric sulfate. The best conditions are as fouows: the mole ratio of methyl alcohol and cinnamic acid is 5:1 (mol/mol), the amount of catalyst is 2.0g, the power of miorwave is 729W, the radiating time of microwave is 3min,the yield was 93.8%. |
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Keywords: | high pressure miorwave methyl cinnamate synthesis catalysis ammonium ferric sulfate |
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