| 西维来司他钠溶剂残留顶空气相色谱法测定的方法学研究 |
| |
| 引用本文： | 唐庆华,胡伟松.西维来司他钠溶剂残留顶空气相色谱法测定的方法学研究[J].福建农林大学学报(哲学社会科学版),2005(2). |
| |
| 作者姓名： | 唐庆华 胡伟松 |
| |
| 作者单位： | 广西桂林制药有限责任公司 桂林541002
(唐庆华)，广西桂林制药有限责任公司 桂林541002(胡伟松) |
| |
| 摘 要： | 建立液固顶空气相色谱法分析西维来司他钠中溶剂残留。采用DB-FFAP大口径毛细管柱,以正丙醇为内标进行定量。正己烷、丙酮、醋酸乙酯、甲醇、乙醇、DMF的回收率分别为96.9%,101.6%,95.4%,101.2%,105.2%,98.7%。最低检测限分别为0.09μg·g-1,0.02μg·g-1,0.08μg·g-1,0.01μg·g-1,0.01μg·g-1,0.16μg·g-1。
|
| 关 键 词： | 西维来司他钠 溶剂残留 气相色谱法 液固顶空气相色谱法 |
Research on the headspace gas chromatography for the determination of residual solvent in Sivelestat Sodium Hydrate |
| |
| Qinghua Tang,Weisong Hu.Research on the headspace gas chromatography for the determination of residual solvent in Sivelestat Sodium Hydrate[J].Journal of Fujian Agriculture and Forestry University,2005(2). |
| |
| Authors: | Qinghua Tang Weisong Hu |
| |
| Abstract: | |
| |
| Keywords: | Sivelestat Sodium Hydrate residual solvent gas chromatography solution-solid ( the two phase balance ) headspace gas chromatography |
| 本文献已被 CNKI 等数据库收录！ |
|
