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黄连须中盐酸小檗碱的提取工艺研究
引用本文:罗音久,曾中良,古淑英.黄连须中盐酸小檗碱的提取工艺研究[J].西南农业大学学报(社会科学版),2002(3).
作者姓名:罗音久  曾中良  古淑英
作者单位:西南农业大学荣昌校区 重庆荣昌402460 (罗音久,曾中良),西南农业大学荣昌校区 重庆荣昌402460(古淑英)
摘    要:根据黄连须中主要有效成分小檗碱易溶于乙醇的性质 ,采用正交设计筛选醇提工艺的最佳条件 ,用紫外分光光度法 ,以提取物中盐酸小檗碱的含量为指标优选提取工艺。结果表明 :黄连须粗粉中加入 5 %的中药提取因子 ,37℃恒温浸泡 6h,乙醇连续回流 3次 ,每次 1h ,总加醇量为2 2倍 ,所得盐酸小檗碱的总量最高 ,提取的盐酸小檗碱总量可达 3.81% ,该工艺为黄连须的更好利用提供了实验依据

关 键 词:黄连须  盐酸小檗碱  提取工艺  中药提取因子

STUDY ON THE EXTRACTION PROCEDURE OF BERBERINE-HYDROCHLORIC FROM FIBROUS RADIX COPTIS
Luo Yinjiu,Zen Zhongliang,Gu Shuying.STUDY ON THE EXTRACTION PROCEDURE OF BERBERINE-HYDROCHLORIC FROM FIBROUS RADIX COPTIS[J].Journal of Southwest Agricultural University:Social Science Edition,2002(3).
Authors:Luo Yinjiu  Zen Zhongliang  Gu Shuying
Institution:Luo Yinjiu Zen Zhongliang Gu Shuying
Abstract:The ethanol extraction procedure, used in extracting berberine-hydrochloric(BBH) from fibrous radix of coptis is described. Optimum conditions were determined as extracted with 5 percent herbal extracting factor, 22 times amounts of ethanol, soaked 6 hours, circumfluence 3 times for 1 hour for every decoction by orthogonal analysis. The results proved that, the extraction procedure were able to obtain 3.81 percent berberine from fibrous radix of coptis.
Keywords:Fibrous radix of coptis  BBH  Extraction procedure  Herbal extracting factor
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