Partial duplication in two-level fractional factorial designs

Most fractional factorial designs have no replicated points and thus do not provide an estimate for pure error. The construction methods for orthogonal main-effect plan in the literature usually do not produce designs with duplicate points. However, it is possible to combine four fractions to provide a set of duplicate points without sacrificing the orthogonality of main effects. This paper proposes two techniques of this idea to produce designs with replicate points in two-level fractional factorial designs.     

Irregular Four-level Response Surface Designs

Four-level response surface designs based on regular two-level fractional factorial designs were introduced by Edmondson (1991). Here, the methods are extended to include designs based on irregular two-level fractional factorials. These designs allow orthogonal blocking and require fewer experimental units than the regular designs.     

Orthogonal three-level parallel flats designs for user-specified resolution

Orthogonal factorial and fractional factorial designs are very popular in many experimental studies, particularly the two-level and three-level designs used in screening experiments. When an experimenter is able to specify the set of possibly nonnegligible factorial effects, it is sometimes possible to obtain an orthogonal design belonging to the class of parallel flats designs, that has a smaller run-size than a suitable design from the class of classical fractional factorial designs belonging to the class of single flat designs. Sri-vastava and Li (1996) proved a fundamental theorem of orthogonal s-level, s being a prime, designs of parallel flats type for the user-specified resolution. They also tabulated a series of orthogonal designs for the two-level case. No orthogonal designs for three-level case are available in their paper. In this paper, we present a simple proof for the theorem given in Srivastava and Li (1996) for the three-level case. We also give a dual form of the theorem, which is more useful for developing an algorithm for construction of orthogonal designs. Some classes of three-level orthogonal designs with practical run-size are given in the paper.     

Designing fractional factorial split-plot experiments with few whole-plot factors

Summary.  When it is impractical to perform the experimental runs of a fractional factorial design in a completely random order, restrictions on the randomization can be imposed. The resulting design is said to have a split-plot, or nested, error structure. Similarly to fractional factorials, fractional factorial split-plot designs can be ranked by using the aberration criterion. Techniques that generate the required designs systematically presuppose unreplicated settings of the whole-plot factors. We use a cheese-making experiment to demonstrate the practical relevance of designs with replicated settings of these factors. We create such designs by splitting the whole plots according to one or more subplot effects. We develop a systematic method to generate the required designs and we use the method to create a table of designs that is likely to be useful in practice.     

On the Use of Semi-folding in Regular Blocked Two-level Factorial Designs

In this article, we consider experimental situations where a blocked regular two-level fractional factorial initial design is used. We investigate the use of the semi-fold technique as a follow-up strategy for de-aliasing effects that are confounded in the initial design as well as an alternative method for constructing blocked fractional factorial designs. A construction method is suggested based on the full foldover technique and sufficient conditions are obtained when the semi-fold yields as many estimable effects as the full foldover.     

On the equivalence of definitions for regular fractions of mixed-level factorial designs

The notion of regularity for fractional factorial designs was originally defined only for two-level factorial designs. Recently, rather different definitions for regular fractions of mixed-level factorial designs have been proposed by Collombier [1996. Plans d’Expérience Factoriels. Springer, Berlin], Wu and Hamada [2000. Experiments. Wiley, New York] and Pistone and Rogantin [2008. Indicator function and complex coding for mixed fractional factorial designs. J. Statist. Plann. Inference 138, 787–802]. In this paper we prove that, surprisingly, these definitions are equivalent. The proof of equivalence relies heavily on the character theory of finite Abelian groups. The group-theoretic framework provides a unified approach to deal with mixed-level factorial designs and treat symmetric factorial designs as a special case. We show how within this framework each regular fraction is uniquely characterized by a defining relation as for two-level factorial designs. The framework also allows us to extend the result that every regular fraction is an orthogonal array of a strength that is related to its resolution, as stated in Dey and Mukerjee [1999. Fractional Factorial Plans. Wiley, New York] to mixed-level factorial designs.     

Switching-one-column follow-up experiments for Plackett-Burman designs

Industrial experiments are frequently performed sequentially using two-level fractional factorial designs. In this context, a common strategy for the design of follow-up experiments is to switch the signs in one column. It is well known that this strategy, when applied to two-level fractional factorial resolution III designs, will clear the main effect, for which the switch was performed, from any confounding with any other two-factor interactions and will also clear all the two-factor interactions between that factor and the other main effects from any confounding with other two-factor interactions. In this article, we extend this result and show that this strategy applies to any orthogonal two-level resolution III design and therefore specifically to any two-level Plackett- Burman design .     

Some new augmented fractional Box–Behnken designs

The augmented Box–Behnken designs are used in the situations in which Box–Behnken designs (BBDs) could not estimate the response surface model due to the presence of third-order terms in the response surface models. These designs are too large for experimental use. Usually experimenters prefer small response surface designs in order to save time, cost, and resources; therefore, using combinations of fractional BBD points, factorial design points, axial design points, and complementary design points, we augment these designs and develop new third-order response surface designs known as augmented fractional BBDs (AFBBDs). These AFBBDs have less design points and are more efficient than augmented BBDs.     

Singular factorial designs resulting from missing pairs of design points

In industry, experiments are often conducted sequentially due to equipment limitations dictating that only one or two simultaneous runs may be made. In this situation, early termination of the experiment results in missing points, leading to a loss in efficiency or, worse, to a singular subdesign with nonestimable model parameters. We investigate the specific problem of singularity when two points are lost from a factorial design based on n two-level factors. The method is based on the inner products of the coordinate vectors of the omitted design points and leads to some results on the nonexistence of fractional factorial designs.     

On the use of partial confounding for the construction of alternative regular two-level blocked fractional factorial designs

In this paper, we consider experimental situations in which a regular fractional factorial design is to be used to study the effects of m two-level factors using n=2^m−k experimental units arranged in 2^p blocks of size 2^m−k−p. In such situations, two-factor interactions are often confounded with blocks and complete information is lost on these two-factor interactions. Here we consider the use of the foldover technique in conjunction with combining designs having different blocking schemes to produce alternative partially confounded blocked fractional factorial designs that have more estimable two-factor interactions or a higher estimation capacity or both than their traditional counterparts.     

Blocking in two-level non-regular fractional factorial designs

In this paper we consider screening experiments where a two-level fractional factorial design is to be used to identify significant factors in an experimental process and where the runs in the experiment are to occur in blocks of equal size. A simple method based on the foldover technique is given for constructing resolution IV orthogonal and non-orthogonal blocked designs and examples are given to illustrate the process.     

Catalogue of Group Structures for Three-level Fractional Factorial Designs

Taguchi (1959) introduced the concept of split-unit design to sort the factors into different groups depending upon the difficulties involved in changing the levels of factors. Li et al. (1991) renamed it as split-plot design. Chen et al. (1993) have given a catalogue of small designs for two- and three-level fractional factorial designs pertaining to a single type of factors. Aggarwal et al. (1997) have given a catalogue of group structure for two-level fractional factorial designs developed under the concept of split-plot design. In this paper, an algorithm has been developed for generating group structure and possible allocations for various 3^n-k fractional factorial designs.     

Minimum Aberration Two-Level Fractional Factorial Split-Plot Designs with Hard to Change Factors

In this article we will consider industrial experiments in which some experimental factors have hard to change levels and others have levels which are easy to change. In such situations, fractional factorial split plot designs are often used where the hard to change factors are included as a subset of the whole plot factors and the easy to change factors make up the subplot factors. Here we consider the problem of finding two-level split plot designs which have minimum aberration among those designs which also minimize the number of level changes for the hard to change factors.     

Supersaturated designs with high searching probability

A supersaturated design is essentially a fractional factorial design whose number of experimental variables is greater than or equal to its number of experimental runs. Under the effect sparsity assumption, a supersaturated design can be very cost-effective. In this paper, our prime objective is to compare the existing two-level supersaturated designs for the noisy case through the probability of correct searching—a powerful criterion proposed by Shirakura et al. [1996. Searching probabilities for nonzeroeffects in search designs for the noisy case. Ann. Statist. 24, 2560–2568]. An algorithm is proposed to construct supersaturated designs with high probability of correct searching. Examples are given for illustration.     

(M,S)-optimality in selecting factorial designs

Use of the (M,S) criterion to select and classify factorial designs is proposed and studied. The criterion is easy to deal with computationally and it is independent of the choice of treatment contrasts. It can be applied to two-level designs as well as multi-level symmetrical and asymmetrical designs. An important connection between the (M,S) and minimum aberration criteria is derived for regular fractional factorial designs. Relations between the (M,S) criterion and generalized minimum aberration criteria on nonregular designs are also discussed. The (M,S) criterion is then applied to study the projective properties of some nonregular designs.     

Mixed two- and four-level fractional factorial split-plot designs with clear effects

Mixed-level designs have become widely used in the practical experiments. When the levels of some factors are difficult to be changed or controlled, fractional factorial split-plot (FFSP) designs are often used. It is highly to know when a mixed-level FFSP design with resolution III or IV has clear effects. This paper investigates the conditions of a resolution III or IV FFSP design with both two-level and four-level factors to have various clear factorial effects, including two types of main effects and three types of two-factor interaction components. The structures of such designs are shown and illustrated with examples.     

Catalogue of group structures for two-level fractional factorial designs

SUMMARY Taguchi introduced the concept of split-unit design to sort factors into different groups with respect to difficulties involved in changing the levels of factors. Li et al. have developed all possible group structures for eight factors in an L16 orthogonal array for resolution IV with split-plot design. Chen et al. have searched for a best design, according to the various criteria for two-level fractional factorial design and have presented a catalogue. In this paper, we have developed an algorithm for generating group structure and possible allocations for various 2n- k fractional factorial designs that correspond to the designs given by Chen et al.     

Indicator function and complex coding for mixed fractional factorial designs

In a general fractional factorial design, the n levels of a factor are coded by the nth roots of the unity. This device allows a full generalization to mixed-level designs of the theory of the polynomial indicator function which has already been introduced for two-level designs in a joint paper with Fontana. The properties of orthogonal arrays and regular fractions are discussed.     

Optimal partially replicated parallel-flats designs for 2×3 mixed factorial experiments

Augmenting additional repeated runs to an unreplicated factorial design provides an economical scheme of obtaining an unbiased estimate for the error variance based on pure replicates. The augmented partially replicated design usually performs satisfactorily in identifying truly active effects regardless of whether the effect sparsity principle holds. Liao and Chai (2009) proposed a set of sufficient conditions for a partially replicated two-level design to be D-optimal over the class of parallel-flats designs. In this article, we generalize their result to the 2^n₁×3^n₂ mixed factorial under D-, A- and E-optimality, and include the 2ⁿ and 3ⁿ symmetric factorials as special cases. In addition, some examples are given to illustrate the main results.     

Optimal block sequences for blocked fractional factorial split-plot designs

It is known that for blocked 2^n-k$2^{n-k}$ designs a judicious sequencing of blocks may allow one to obtain early and insightful results regarding influential parameters in the experiment. Such findings may justify the early termination of the experiment thereby producing cost and time savings. This paper introduces an approach for selecting the optimal sequence of blocks for regular two-level blocked fractional factorial split-plot screening experiments. An optimality criterion is developed so as to give priority to the early estimation of low-order factorial effects. This criterion is then applied to the minimum aberration blocked fractional factorial split-plot designs tabled in McLeod and Brewster [2004. The design of blocked fractional factorial split-plot experiments. Technometrics 46, 135–146]. We provide a catalog of optimal block sequences for 16 and 32-run minimum aberration blocked fractional factorial split-plot designs run in either 4 or 8 blocks.