On Some Chemical Balance Weighing Designs

The present paper deals with certain chemical balance weighing designs. The incidence matrices of BIB designs and balanced ternary designs have been used to construct these designs. Conditions have been obtained to make some of these designs “optimum”.     

OPTIMUM SINGULAR SPRING BALANCE WEIGHING DESIGNS WITH NON-HOMOGENEITY OF THE VARIANCES OF ERRORS FOR ESTIMATING THE TOTAL WEIGHT

The problem of estimation of the total weight of objects using a singular spring balance weighing design with non-homogeneity of the variances of errors has been dealt with in this paper. Based on a theorem by Katulska (1984) giving a lower bound for the variance of the estimated total weight, a necessary and sufficient condition for this lower bound to be attained is obtained. It is shown that weighing designs for which the the lower bound is attainable, can be constructed from the incidence matrices of (α₁,.,α_t)-resolvable block designs, α-resolvable block designs, singular group divisible designs, and semi-regular group divisible designs.     

Regular E-Optimal Spring Balance Weighing Designs with Correlated Errors

The problems linked with an E-optimal spring balance weighing design with correlated errors are discussed. The topic is focus on the determining the maximal eigenvalue of the inverse of the information matrix of estimators. The constructing method of the E-optimal design, based on the incidence matrices of balanced incomplete block designs, is presented.     

Use of balanced bipartite weighing designs as chemical balance designs

This paper deals with the use of balanced bipartite weighing designs as chemical balance designs when there Is a restriction on the number of objects that can be placed on either pan..The variance of each estimated weight and the covarlance of each pair of estimated weights are worked out.The use of additional weighing when the design matrix is singular is discussed.     

Efficiency balanced designs through reinforcement

In this investigation, general efficiency balanced (GEB) and efficiency balanced (EB) designs with (v + t) treatments, using (i) balanced incomplete block (BIB), (ii) symmetrical BIB, (iii) f -resolvable BIB, (iv) group divisible (GD) and (v) resolvable GD designs have been constructed with smaller number of replications and block sizes.     

On a class of variance balanced incomplete block designs

In this paper variance balanced incomplete block designs have been constructed for situations when suitable BIB designs do not exist for a given number of treatments, because of the contraints bk=vr, λ(v-1) = r(k-l). These variance balanced designs are in unequal block sizes and unequal replications.     

On the optimality of chemical balance weighing designs

In this paper we consider the problem of optimally weighing n objects with N weighings on a chemical balance. Several previously known results are generalized. In particular, the designs shown by Ehlich (1964a) and Payne (1974) to be D-optimal in various classes of weighing designs where N≡2 (mod4) are shown to be optimal with respect to any optimality criterion of Type I as defined in Cheng (1980). Several results on the E-optimality of weighing designs are also given.     

Regular A-optimal design matrices X = (xij) with xij = ?1, 0, 1

New construction methods of the regular A-optimal design matrices with elements −1, 0, 1 are presented, under assumption of nonhomogeneity of variance error. The presented constructions are based on the incidence matrices of the balanced bipartite weighing designs.     

Efficient three-level screening designs using weighing matrices

Screening is the first stage of many industrial experiments and is used to determine efficiently and effectively a small number of potential factors among a large number of factors which may affect a particular response. In a recent paper, Jones and Nachtsheim [A class of three-level designs for definitive screening in the presence of second-order effects. J. Qual. Technol. 2011;43:1–15] have given a class of three-level designs for screening in the presence of second-order effects using a variant of the coordinate exchange algorithm as it was given by Meyer and Nachtsheim [The coordinate-exchange algorithm for constructing exact optimal experimental designs. Technometrics 1995;37:60–69]. Xiao et al. [Constructing definitive screening designs using conference matrices. J. Qual. Technol. 2012;44:2–8] have used conference matrices to construct definitive screening designs with good properties. In this paper, we propose a method for the construction of efficient three-level screening designs based on weighing matrices and their complete foldover. This method can be considered as a generalization of the method proposed by Xiao et al. [Constructing definitive screening designs using conference matrices. J. Qual. Technol. 2012;44:2–8]. Many new orthogonal three-level screening designs are constructed and their properties are explored. These designs are highly D-efficient and provide uncorrelated estimates of main effects that are unbiased by any second-order effect. Our approach is relatively straightforward and no computer search is needed since our designs are constructed using known weighing matrices.     

Complete diallel crosses plans through balanced incomplete block designs

The present investigation involves the methods of construction of complete diallel cross plans using balanced incomplete block (BIB) designs. Furthermore, the analysis of complete diallel crosses plans are carried out to estimate the general combining ability of the ith line (i=1, r 2, r …, r v) where the intra- block analysis of the adjusted sum of squares for GCA and the unadjusted block sum of squares are also obtained, thereafter the relationship between the estimates of BIB design and the estimates of the GCA effect of CDC plan has been established. Moreover, it has also been shown that the complete diallel crosses design obtained through two BIB designs satisfying v1=b1= 4 5 1+3=v2=b2, r r1=2 5 1+1=r2=k1=k2 and 5 1= 5 2 are universally optimum. These results are further supported by a suitable example of each. However, the need of this study is to show that the analysis of the CDC plan is reducible to the analysis of generating the BIB design.     

Mixture designs with orthogonal blocks

Constructions of blocked mixture designs are considered in situations where BLUEs of the block effect contrasts are orthogonal to the BLUEs of the regression coefficients. Orthogonal arrays (OA), Balanced Arrays (BAs), incidence matrices of balanced incomplete block designs (BIBDs), and partially balanced incomplete block designs (PBIBDs) are used. Designs with equal and unequal block sizes are considered. Also both cases where the constants involved in the orthogonality conditions depend and do not depend on the factors have been taken into account. Some standard (already available) designs can be obtained as particular cases of the designs proposed here.     

D-optimal weighing designs and optimal chemical balance weighing designs for estimating the total weight

This paper provides D-optimal spring balance designs for estimating individual weights when the number of objects to be weighed in each weighing, B, is fixed. D-optimal chemical balance designs for estimating total weight under both homogeneous and nonhomogeneous error variances are found when the number of objects weighed in each weighing is ≥ B, a fixed number.

We indicate the restriction used in Chacko & Dey(1978) and Kageyama(1988), i.e. that chemical designs X be restricted to designs in which exactly “a” objects are replaced on the left pan and exactly “b” on the right pan in each of the weighings for a, b > 0, is unnecessary.     

PARTIALLY EQUINEIGHBOURED DESIGNS

This paper presents further results on a class of designs called equineighboured designs, ED. These designs are intended for field and related experiments, especially whenever there is evidence that observations in the same block are correlated. An ED has the property that every unordered pair of treatments occurs as nearest neighbours equally frequently at each level. Ipinyomi (1986) has defined and shown that ED are balanced designs when neighbouring observations are correlated. He has also presented ED as a continuation of the development of optimal block designs. An ED would often require many times the number of experimental materials needed for the construction of an ordinary balanced incomplete block, BIB, design for the same number of treatments and block sizes. Thus for a relatively large number of treatments and block sizes the required minimum number of blocks may be excessively large for practical use of ED. In this paper we shall define and examine partially equineighboured designs with n concurrences, PED (n), as alternatives where ED are practically unachievable. Particular attention will be given to designs with smaller numbers of blocks and for which only as little balance as possible may be lost.     

CONSTRUCTION OF BALANCED TERNARY DESIGNS

In this paper variance balanced ternary designs are constructed in unequal block sizes for situations when suitable BIB designs do not exist for a given number of treatments because of the constraints bk=vr,and λ(v - 1) =r(k- 1).     

Balanced and partially balanced incomplete block designs with autocorrelation errors

The paper aims to find variance balanced and variance partially balanced incomplete block designs when observations within blocks are autocorrelated and we call them BIBAC and PBIBAC designs. Orthogonal arrays of type I and type II when used as BIBAC designs have smaller average variance of elementary contrasts of treatment effects compared to the corresponding Balanced Incomplete Block (BIB) designs with homoscedastic, uncorrelated errors. The relative efficiency of BIB designs compared to BIBAC designs depends on the block size k and the autocorrelation ρ and is independent of the number of treatments. Further this relative efficiency increases with increasing k. Partially balanced incomplete block designs with autocorrelated errors are introduced using partially balanced incomplete block designs and orthogonal arrays of type I and type II.     

Use of n-ary block designs in diallel crosses evaluation

To fill the gap between theory and practice of modern statistical designs, this paper presents the use of n-ary block designs in the evaluation of balanced incomplete block (BIB) designs for all the four Griffing's (1956) complete dialled crosses (CDC) systems, the construction of which is proposed here by adopting a suitable BIB design and associating its treatments with the crosses under a CDC system.     

ON THE ESTIMATION OF TOTAL WEIGHT IN SINGULAR SPRING BALANCE WEIGHING DESIGNS UNDER THE CO VARIANCE MATRIX OF ERRORS s2G

The problem of the estimation of the linear combination of weights, c′w, in a singular spring balance weighing design when the error structure takes the form E(ee′) =s?²G has been studied. A lower bound for the variance of the estimated linear combination of weights is obtained and a necessary and sufficient condition for this lower bound to be attained is given. The general results are applied to the case of the total of the weights. For a specified form for G, some optimum spring balance weighing designs for the estimated total weight are found.     

On some properties of the dual of a totally balanced block design

In this paper it is shown that the dual of a totally balanced block design with t = b, is also a totally balanced block design. It is shown that Fisher's inequality $\text{b≧t}$ for BIB designs, holds also for a totally balanced block design.     

Optimum chemical balance weighing designs for estimating the total weight

This deals with chemical balance weighing designs which attain a lower bound for the variance of the estimated total weight, The results extend those of Chacko Dey (1978).     

Recent developments in D-optimal designs

In the paper, some issues concerned with the determining spring balance weighing designs satisfying the criterion of D-optimality under the assumption measurement errors are uncorrelated and they have the same variances are discussed. In addition, highly D-efficient spring balance weighing designs are also considered. Some conditions under which any spring balance weighing design is regular D-optimal or highly D-efficient are proved. What is more, new construction methods of regular D-optimal and highly D-efficient spring balance weighing designs are presented.