Designing fractional factorial split-plot experiments with few whole-plot factors

Summary.  When it is impractical to perform the experimental runs of a fractional factorial design in a completely random order, restrictions on the randomization can be imposed. The resulting design is said to have a split-plot, or nested, error structure. Similarly to fractional factorials, fractional factorial split-plot designs can be ranked by using the aberration criterion. Techniques that generate the required designs systematically presuppose unreplicated settings of the whole-plot factors. We use a cheese-making experiment to demonstrate the practical relevance of designs with replicated settings of these factors. We create such designs by splitting the whole plots according to one or more subplot effects. We develop a systematic method to generate the required designs and we use the method to create a table of designs that is likely to be useful in practice.     

Mixed two- and four-level fractional factorial split-plot designs with clear effects

Mixed-level designs have become widely used in the practical experiments. When the levels of some factors are difficult to be changed or controlled, fractional factorial split-plot (FFSP) designs are often used. It is highly to know when a mixed-level FFSP design with resolution III or IV has clear effects. This paper investigates the conditions of a resolution III or IV FFSP design with both two-level and four-level factors to have various clear factorial effects, including two types of main effects and three types of two-factor interaction components. The structures of such designs are shown and illustrated with examples.     

Optimal block sequences for blocked fractional factorial split-plot designs

It is known that for blocked 2^n-k$2^{n-k}$ designs a judicious sequencing of blocks may allow one to obtain early and insightful results regarding influential parameters in the experiment. Such findings may justify the early termination of the experiment thereby producing cost and time savings. This paper introduces an approach for selecting the optimal sequence of blocks for regular two-level blocked fractional factorial split-plot screening experiments. An optimality criterion is developed so as to give priority to the early estimation of low-order factorial effects. This criterion is then applied to the minimum aberration blocked fractional factorial split-plot designs tabled in McLeod and Brewster [2004. The design of blocked fractional factorial split-plot experiments. Technometrics 46, 135–146]. We provide a catalog of optimal block sequences for 16 and 32-run minimum aberration blocked fractional factorial split-plot designs run in either 4 or 8 blocks.     

Identification of factors influencing dispersion in split-plot experiments

As split-plot designs are commonly used in robust design it is important to identify factors in these designs that influence the dispersion of the response variable. In this article, the Bergman-Hynén method, developed for identification of dispersion effects in unreplicated experiments, is modified to be used in the context of split-plot experiments. The modification of the Bergman-Hynén method enables identification of factors that influence specific variance components in unreplicated two-level fractional factorial splitplot experiments. An industrial example is used to illustrate the proposed method.     

Designing fractional two-level experiments with nested error structures

A common feature of experiments with a random blocking factor and splitplot experiments is their nested error structure. This paper proposes a general strategy to handle fractional two-level experiments with such error structures. The strategy aims to create error strata with sufficient numbers of contrasts to separate active effects from inactive effects. The strategy also details the construction of treatment generators, given the constraints of a predetermined error structure. The key elements of the strategy are illustrated with a chemical experiment that has 16 factors and 32 runs blocked according to working days, and a cheese-making experiment that has 11 factors and 128 runs, divided over milk supplies as whole plots, curds productions as subplots and sets of identically treated cheeses as sub-subplots.     

Fixing a factor in the sequential design of two-level fractional factorial experiments

When designing two-level fractional factorial experiments sequentially, there is a wide choice of designs that could be used at each stage. Designs in which one of the factors is fixed at a particular level after the first experiment are studied in this paper. This sometimes allows all important effects to be estimated in fewer runs than would the standard sequences of designs, and effects can sometimes be estimated more efficiently. The properties of some sequences are presented, and extensions to fixing more than one factor and to factors with more than two levels are discussed.     

Designing selection experiments with bernoulli populations

This paper is concerned with a fixed size subset selection problem for Bernoulli populations in the framework of the indifference zone approach. The goal is to select s populationswhich contain at least c of those with the t largest success probabilities. In order to control the probability of correct selection over the preference zone extensive tables of exact minimum sample sizes have been prepared to implement the single-stage procedure generalized from the well-known Sobel-Huyett procedure. It is shown how the tables can also be employed to design certain closedsequential procedures. These procedures curtail the sampling process of the single-stage procedureand may differ in their sampling rules. Two procedures working with play-the-winner rules are described in detail     

Equivalence of factorial designs with qualitative and quantitative factors

Two symmetric fractional factorial designs with qualitative and quantitative factors are equivalent if the design matrix of one can be obtained from the design matrix of the other by row and column permutations, relabeling of the levels of the qualitative factors and reversal of the levels of the quantitative factors. In this paper, necessary and sufficient methods of determining equivalence of any two symmetric designs with both types of factors are given. An algorithm used to check equivalence or non-equivalence is evaluated. If two designs are equivalent the algorithm gives a set of permutations which map one design to the other. Fast screening methods for non-equivalence are considered. Extensions of results to asymmetric fractional factorial designs with qualitative and quantitative factors are discussed.     

Optimal fractional factorial designs for estimating interactions of one factor with all others: 3m Series

In some experimental situations, only one factor is expected to interact with other factors. Designs which permit estimation of all main effects and the interactions of one factor ‘With All Others’, are termed WAO designs. This paper discusses the existence and construction of s^m WAO designs. A series of WAO designs are presented for the 3^m factorial, for m = 6, 7, ... , 14. The p non-negligible effects are estimable in 9f^? runs, where f^? is the smallest integer such that 9f^? ≥p. These designs are determinant optimal within the class of parallel flats fractions and, except for the case f^? = 9, are new. They are ideally suited for sequential experiments.     

Determination of optimum experimental conditions using dispersion main effects and interactions of factors in replicated factorial experiments

Dispersion main effects and two-factor interactions are first defined and then estimated in replicated factorial experiments. A method based on Union-Intersection rules, using dispersion main effects and two factor interactions is proposed for finding the level combinations of control factors so that the response variability due to noise is minimum. Illustrative examples are also given.     

Block designs for incomplete factorial treatment structures with two factors

Abstract

In this paper, the problem of obtaining efficient block designs for incomplete factorial treatment structure with two factors excluding one treatment combination for estimation of dual versus single treatment contrasts is considered. The designs have been obtained using the A-optimal completely randomized designs and modified strongest treatment interchange algorithm. A catalog of efficient block designs has been prepared for m₁?=?3, 4 and m₂?=?2, b?≤?10 and k?≤?9 and for m₁?=?3,4 and m₂?=?3, 4, b?≤?10 and k?≤?10.     

Mixed covering arrays of strength three with few factors

Covering arrays with mixed alphabet sizes, or mixed covering arrays, are useful generalizations of covering arrays that are motivated by software and network testing. Suppose that there are k factors, and that the ith factor takes values or levels from a set G_i of size g_i. A run is an assignment of an admissible level to each factor. A mixed covering array, MCA(N;t,k,g₁g₂…g_k), is a collection of N runs such that for any t distinct factors, i₁,i₂,…,i_t, every t-tuple from G_i1×G_i2×?×G_it occurs in factors i₁,i₂,…,i_t in at least one of the N runs. When g=g₁=g₂=?=g_k, an MCA(N;t,k,g₁g₂…g_k) is a CA(N;t,k,g). The mixed covering array number, denoted by MCAN(t,k,g₁g₂…g_k), is the minimum N for which an MCA(N;t,k,g₁g₂…g_k) exists. In this paper, we focus on the constructions of mixed covering arrays of strength three. The numbers MCAN(3,k,g₁g₂…g_k) are determined for all cases with k∈{3,4} and for most cases with k∈{5,6}.     

Designs for two-level factorial experiments with linear models containing main effects and selected two-factor interactions

An orthogonal polynomial model is used to model the response influenced by n two level factors. Such a model is represented by an undirected graph g with n vertices and e edges. The vertices identify the n main effects and the e edges identify the two-factor interactions of interest which together with the mean are the parameters of interest. A g-design is a saturated design which can provide an unbiased estimator for these parameters and its design matrix is called a g-matrix. The latter two concepts were introduced by Hedayat and Pesotan (Statistica Sinica 2 (1992), 453–464). In this paper methods of constructing g-matrices are studied since such constructions are equivalent to the construction of g-designs. Some bounds on the absolute value of a determinant of a g-matrix are given and D-optimality results on certain classes of g-matrices are presented.     

Characterization of singular balanced fractional sm factorial designs derivable from balanced arrays with maximum number of constraints

An upper bound on the maximum number of constraints for s-symbol balanced arrays is derived. It is shown that balanced fractional s^m factorial designs derived from some balanced arrays with the maximum possible number of constraints become singular.     

Designing completely randomized experiments to detect ordered treatment effects: an empirical study

In designing experiments the researcher frequently must decide as to how to allocate fixed resources among k factor levels (Cox (1958)). This study investigates the effects on the power of a test caused by changes in: the sample size (n); the number of factor levels (k); the allocation of fixed total observations (N) among k and n: the shift parameter (ø); the type of parent population sampled; and, the type of ordered location alternative involved. Using Monte Carlo methods the powers of eight test procedures specifically devised to detect ordered treatment effects under completely randomized designs were evaluated along with those of the more general one-way F test. The results are of interest to researchers in all fields of application.     

Optimal design of complex experiments with qualitative factors of influence

A complex experiment with qualirarive factors influencing the outcome of the experiment can be seen as a general ANOVA setup. A design of such an experiment will be the assignment at which of the possible levels of the factors the actual experiment should be performed. In this paper optimal designs of such experiments will be characterized with respect to three different optimality criteria including the so called uniform optimality of a design. The possible applications of the main optimization result providing these characterizations can be used to more general experiments. The particular results on these generalizations will be indicated at the end of this paper.