| 乙酰二茂铁的合成与性质测定 |
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| 引用本文： | 卓馨.乙酰二茂铁的合成与性质测定[J].宿州学院学报,2006,21(6):97-99,120. |
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| 作者姓名： | 卓馨 |
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| 作者单位： | 宿州学院光电实验室,安徽,宿州,234000 |
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| 基金项目： | 宿州学院教学研究项目(JY2007033)。 |
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| 摘 要： | 利用二茂铁的酰化反应原理对合成乙酰二茂铁的工艺进行了研究,探讨了反应温度、催化剂用量及投料方式对合成工艺的影响。通过红外光谱和紫外光谱对乙酰二茂铁进行表征,测定了合成的乙酰二茂铁的熔点,并用循环伏安法测定乙酰二茂铁的电化学性质。
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| 关 键 词： | 二茂铁 乙酰二茂铁 酰化 |
| 文章编号： | 1673-2006(2006)06-0097-03 |
| 修稿时间： | 2006年5月20日 |
The Preparation and Characterization of Acetylferrocene |
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| ZHUO Xin.The Preparation and Characterization of Acetylferrocene[J].Journal of Shuzhou College,2006,21(6):97-99,120. |
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| Authors: | ZHUO Xin |
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| Abstract: | The technology of synthesizing acetylferrocene by the react principle of the acetylation of ferrocene was discussed.The influence of the react temperature,the quantity of the catalyst,the charging of reactants on the synthetic technology were investigated.The alkylferrocenes were characterized by IR spectrum and CV spectrum.Melting point of acetylferrocene were determined.The electrochemical properties of acetylferrocene were investigated by cyclic voltammetry. |
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| Keywords: | Ferrocene Acetylferrocene Acidulation |
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