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在线消解流动注射光度法测定水中的总磷
引用本文:赵萍,陈金辉,肖靖泽.在线消解流动注射光度法测定水中的总磷[J].福建农林大学学报(哲学社会科学版),2007(4).
作者姓名:赵萍  陈金辉  肖靖泽
作者单位:北京吉天仪器有限公司 北京100016
基金项目:国家科技部"十五"科技攻关项目(编号:2004BA210A05)。
摘    要:使用自行研制的全自动流动注射分析仪,采用在线消解流动注射法测定水中的总磷。方法的检出限为0.008mg/LP;线性范围为0.1-5mg/LP,线性相关系数r为0.9998;其相对标准偏差为0.69%;实际水样的加标回收率为93%-111%;样品测定频率为14样/小时。本方法快速、简便、灵敏度较高,线性范围、精密度和准确度均符合国家标准。

关 键 词:流动注射分析  在线消解  总磷

Determination of Total phosphate in Water by on-Line Digestion Flow Injection Analysis
Zhao Ping,Chen Jinghui,Xiao Jingze Beijing Titan Instruments Co.,Ltd.Determination of Total phosphate in Water by on-Line Digestion Flow Injection Analysis[J].Journal of Fujian Agriculture and Forestry University,2007(4).
Authors:Zhao Ping  Chen Jinghui  Xiao Jingze Beijing Titan Instruments Co  Ltd
Institution:Zhao Ping,Chen Jinghui,Xiao Jingze Beijing Titan Instruments Co.,Ltd.Beijing,100016 F/4,Bldg M6,No.1 Jiuxianqiao East Road,Chaoyang District,Beijing,100016
Abstract:Total phosphate in water was determined by using on-line digestion flow injection analysis method using automated flow injection analyzer developed by Titan Intruments.The detection limit was 0.008mg/L P and the liner range was 0.1-5mg/L P(r=0.9998).The relative standard deviation was 0.69% and the recovery was 93%-111%.The method is rapid,simple,sensitive,the linear range,precision and accuracy all consist with GB standard.
Keywords:flow injection analysis  on-line digestion  total phosphate
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