| N1-正十二烷基二乙烯三胺的合成和生物活性研究 |
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| 引用本文： | 刘璐,刘希光,董向丽,刘刚,徐胜广,唐晓红. N1-正十二烷基二乙烯三胺的合成和生物活性研究[J]. 鲁东大学学报, 2013, 0(1): 51-53,65 |
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| 作者姓名： | 刘璐 刘希光 董向丽 刘刚 徐胜广 唐晓红 |
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| 作者单位： | 鲁东大学化学与材料科学学院;青岛农业大学农学与植物保护学院 |
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| 基金项目： | 山东省自然科学基金(ZR2009BL014);鲁东大学校科研基金(LZ20082903) |
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| 摘 要： | 以二乙烯三胺和正溴十二烷为原料，合成了N1-正十二烷基二乙烯三胺衍生物，并用红外光谱与核磁共振氢谱对其结构进行了表征．初步的活性实验结果表明：N1-正十二烷基二乙烯三胺衍生物对苹果腐烂病菌及苹果轮纹病菌均表现出极好的抑制活性，对两种病原真菌的Ec50分别为36．15μg／mL和26．22μg／mL．
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| 关 键 词： | 二乙烯三胺 合成 杀菌活性 生长速率法 |
The Study on the Synthesis and Biological Activity of N1-dodecyl diethylentriamine |
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| LIU Lu,LIU Xi-guang,DONG Xiang-li,LIU Gang,XU Sheng-guang,TANG Xiao-hong. The Study on the Synthesis and Biological Activity of N1-dodecyl diethylentriamine[J]. Ludong University Journal (Natural Science Edition), 2013, 0(1): 51-53,65 |
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| Authors: | LIU Lu LIU Xi-guang DONG Xiang-li LIU Gang XU Sheng-guang TANG Xiao-hong |
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| Affiliation: | 1(1.School of Chemistry and Materials Science,Ludong University,Yantai 264039,China; 2.College of Agronomy and Plant Protection,Qingdao Agricultural University,Qingdao 266109,China) |
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| Abstract: | N1-dodecyl diethylentriamine derivative was synthesized by the reaction of diethylentriamine with 1- bromododecane, and its structure was characterized by using infrared spectrum and 1H-NMR spectroscopy. The preliminary bioassay results showed that the N1-dodecyl diethylentriamine exhibited good fungicidal activity, and the EC50 value of N1-dodecyl diethylentriamine was reached 36. 15 μg/mL and 26. 22 μg/mL against Valsa mall and Physalospora piricola. |
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| Keywords: | diethylentriamine synthesis fungicidal activity growth rate method |
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