| 高效液相色谱法测定芩黄喉症胶囊中栀子苷的含量 |
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| 引用本文： | 焦少珍,赵建芬,梁巧荣.高效液相色谱法测定芩黄喉症胶囊中栀子苷的含量[J].肇庆学院学报,2009,30(2):37-39. |
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| 作者姓名： | 焦少珍 赵建芬 梁巧荣 |
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| 作者单位： | 1. 肇庆学院生命科学学院,广东,肇庆,526061
2. 肇庆学院化学化工学院,广东,肇庆,526061 |
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| 基金项目： | 肇庆学院青年科学研究基金 |
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| 摘 要： | 建立了芩黄喉症胶囊中栀子苷含量的测定方法.色谱分析条件如下：采用Agilent Eclipse XDB-C18柱,以甲醇-水溶液（25：75）为流动相,流速为1 mL/min,柱温为室温,检测波长为240 nm,栀子苷的线性范围为4.8～19.2μg/mL,r=0.999 0.平均加标回收率为100.6%,相对标准偏差为1.1%.
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| 关 键 词： | 高效液相色谱法 芩黄喉症胶囊 栀子苷 |
Determination of Geniposide in Qinhuang Houzheng Capsule by HPLC |
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| JIAO Shaozhen,Zhao Jianfen,Liang Qiaorong.Determination of Geniposide in Qinhuang Houzheng Capsule by HPLC[J].Journal of Zhaoqing University (Bimonthly),2009,30(2):37-39. |
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| Authors: | JIAO Shaozhen Zhao Jianfen Liang Qiaorong |
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| Institution: | (a.Faeulty of Life Sciences; b. Faculty of Chemistry and Chemical Engineering,Zhaoqing University,Zhaoqing Guangdong 526061 ,China) |
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| Abstract: | A phase high performance liquid chromatography for the determination of geniposide in Qinhuang Houzheng capsule is established. The optimum chromatographic conditions were as follows： Agilent Eclipse XDB-C18 column was made use as the column,methanol-H2O was used as mobile phase. The flow rate was 1mL/min. The column temperature was at room temperature. The detection wavelength was 240 nm. The result showed that the linear range of geniposide was in the range of 4.8-19.2 μg/mL,r =0.999 0, the average recovery was 100.6 %,RSD=1. 1%. |
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| Keywords: | HPLC Qinhuang Houzheng capsule geniposide |
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